Response surface optimization of SPME extraction conditions for the analysis of volatile compounds in Brazilian sugar cane spirits by HS‐SPME-GC-MS

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dc.creatorZacaroni, Lidiany Mendonça
dc.creatorSales, Priscila Ferreira de
dc.creatorCardoso, Maria das Graças
dc.creatorSantiago, Wilder Douglas
dc.creatorNelson, David Lee
dc.date.accessioned2018-12-28T16:04:18Z
dc.date.available2018-12-28T16:04:18Z
dc.date.issued2017
dc.description.abstractThe extraction of volatile compounds from distilled sugarcane spirits was investigated using central composite design associated with response surface methodology. The parameters evaluated were the extraction temperature, extraction time and desorption time. All of the parameters analysed, as well as their interactions, were significant for the process at a 95% confidence level. Although the extraction time and extraction temperature exhibited positive effects, the desorption time showed a negative effect. The second‐order polynomial model was adjusted appropriately for the response surface analysis. The optimized conditions were extraction temperature equal to 45°C, extraction time of 50 min and the desorption time corresponding to 100 s. Copyright © 2017 The Institute of Brewing & Distillingpt_BR
dc.identifier.citationZACARONI, L. M. et al. Response surface optimization of SPME extraction conditions for the analysis of volatile compounds in Brazilian sugar cane spirits by HS‐SPME-GC-MS. Journal of The Institute of Brewing, London, v. 123, n. 2, p. 226-231, 2017.pt_BR
dc.identifier.urihttps://repositorio.ufla.br/handle/1/32338
dc.identifier.urihttps://onlinelibrary.wiley.com/doi/full/10.1002/jib.410pt_BR
dc.languageen_USpt_BR
dc.publisherThe Institute of Brewing & Distillingpt_BR
dc.rightsrestrictAccesspt_BR
dc.sourceJournal of The Institute of Brewingpt_BR
dc.subjectVolatile compoundspt_BR
dc.subjectDistilled sugarcane spiritspt_BR
dc.subjectSolid‐phase microextractionpt_BR
dc.subjectResponse surface methodpt_BR
dc.subjectCompostos voláteispt_BR
dc.subjectAguardente de cana destiladapt_BR
dc.subjectMicroextração em fase sólidapt_BR
dc.subjectMétodo de superfície de respostapt_BR
dc.titleResponse surface optimization of SPME extraction conditions for the analysis of volatile compounds in Brazilian sugar cane spirits by HS‐SPME-GC-MSpt_BR
dc.typeArtigopt_BR

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